AATCC TM162-2011e2 Test Method for Colorfastness to Water Chlorinated Pool 耐水色牢度试验方法：氯化池

VIP免费

那山那人那狗 2025-04-27 13 209.84KB 2 页 15星币

侵权投诉

314 AATCC TM162-2011e2 AATCC Manual of International Test Methods and Procedures/2023

Developed in 1984 by Committee RA23.

Supersedes AATCC TM105-1975; edito-

rially revised 1985, 1995, 2008, 2010,

2012, 2019; editorially revised and re-

affirmed 1986, 1997; reaffirmed 1991,

2002, 2009; revised 2011. Related to

ISO 105-E03.

1. Purpose and Scope

1.1 This test method is used for evalu-

ating the resistance to chlorinated pool

water of dyed, printed or otherwise col-

ored textile yarns and fabrics of all kinds.

2. Principle

2.1 Yarn or fabric specimens are agi-

tated at a fixed rate in diluted chlorine so-

lution under specified conditions of tem-

perature, time, pH and hardness. The

dried specimens are evaluated for change

in color.

3. Terminology

3.1 colorfastness, n.—the resistance of

a material to change in any of its color

characteristics, to transfer of its colo-

rant(s) to adjacent materials or both, as a

result of the exposure of the material to

any environment that might be encoun-

tered during the processing, testing, stor-

age or use of the material.

3.2 pool water, n.—water to which

various chemicals are added to maintain

purity and clarity, normally used for

swimming.

4. Precautions

NOTE: These safety precautions are

for information purposes only. The pre-

cautions are ancillary to the testing proce-

dures and are not intended to be all inclu-

sive. It is the user’s responsibility to use

safe and proper techniques in handling

materials in this test method. Manufac-

turers MUST be consulted for specific

details such as material safety data sheets

and other manufacturer’s recommenda-

tions. All OSHA standards and rules

must also be consulted and followed.

4.1 Good laboratory practices should

be followed. Wear safety glasses in all

laboratory areas.

4.2 All chemicals should be handled

with care.

4.3 When using 6N sulfuric acid and

acetic acid, use chemical goggles or face

shield, impervious gloves and an imper-

vious apron. Concentrated acids should

be handled only in an adequately venti-

lated laboratory hood. CAUTION: Al-

ways add acid to water.

4.4 An eyewash/safety shower should

be located nearby and a high efficiency

particulate respirator with a full face-

piece should be readily available for

emergency use.

4.5 Manufacturer’s safety recommen-

dations should be followed when operat-

ing laboratory testing equipment.

4.6 Observe padder safety. Ensure ade-

quate guard at the nip point. Normal safe-

guards on pad should not be removed. A

foot-operated kickoff is recommended.

4.7 Exposure to chemicals used in this

procedure must be controlled at or below

levels set by governmental authorities

(e.g., Occupational Safety and Health

Administration’s [OSHA] permissible ex-

posure limits [PEL] as found in 29 CFR

1910.1000; see web site: www.osha.gov

for latest version). In addition, the Ameri-

can Conference of Governmental Indus-

trial Hygienists (ACGIH) Threshold

Limit Values (TLVs) comprised of time

weighted averages (TLV-TWA), short

term exposure limits (TLV-STEL) and

ceiling limits (TLV-C) are recommended

as a general guide for air contaminant ex-

posure which should be met (see 11.1).

5. Apparatus and Materials (see 11.2)

5.1 Equipment:

5.1.1 Option 1-Accelerated laundering

machine (see 7.1 and 11.3).

5.1.2 Stainless steel lever lock canis-

ters Type 2, 1200 mL, 90 × 200 mL (3.5

× 8.0 in.).

5.2 Option 2-Drycleaning Cylinder

(see 7.2 and 11.4).

5.3 Wringer.

5.4 Gray Scale for Color Change

(AATCC EP1) (see 11.6).

5.5 Test Control Fabric 162 (see 11.6).

5.6 Reagents:

5.6.1 Household sodium hypochlorite

solution (NaOCl), approximately 5%

available chlorine (see 11.5).

5.6.2 Calcium chloride, anhydrous

(CaCl2).

5.6.3 Magnesium chloride, hexahy-

drate (MgCl2 · 6H2O).

5.6.4 Sulfuric acid (H2SO4), 6N.

5.6.5 Potassium iodide, KI, 12%.

5.6.6 Starch solution, 1%.

5.6.7 Sodium thiosulfate (Na2S2O3),

0.01N, (see 11.7).

5.6.8 Distilled or deionized water.

5.6.9 Sodium carbonate (Na2CO3).

5.6.10 Acetic acid (CH3COOH).

6. Preparation of Reagents

6.1 Deionized or distilled water to

which 5 ppm chlorine and 100 ppm salts

(hardness concentrate) are added; ad-

justed to 21°C (70°F) and pH 7.0 with

sodium carbonate or acetic acid.

7. Test Specimens

7.1 Option 1-Accelerated Laundering

Machine.

7.1.1 Specimen size 5 × 5 cm; control

fabric size 5 × 5 cm. Total weight of spec-

imen and control fabric 1.0 ± 0.05 g.

Multiple specimens of the same sample

can be used to achieve a 1.0 g load.

7.2 Option 2-Drycleaning Cylinder

Equipment.

7.2.1 Colored specimens, approxi-

mately 6 × 6 cm. Total weight of test

specimens should be 5.0 ± 0.25 g. If

specimens to be tested do not weigh 5.0

g, add multiple specimens to make 5.0 g.

Include the Test Control Fabric in the 5.0

g weight. Different colored specimens

can be mixed when making up the 5.0 g

load.

8. Procedure

8.1 Solution Preparation.

8.1.1 Add 800 mL deionized or dis-

tilled water to a 1 L volumetric flask and

add 8.24 g calcium chloride and 5.07 g

magnesium chloride while stirring to dis-

solve. Bring volume up to 1 L with water.

This is a “hardness concentrate” which

can be retained and used for 30 days.

8.1.2 Dilute 51 mL hardness concen-

trate to 5100 mL with deionized or dis-

tilled water. Add 0.5 mL household so-

dium hypochlorite solution which is no

more than 60 days old. Determine actual

ppm Cl by titration and adjust to 5 ppm

(see 11.7).

8.1.3 0.01N Sodium thiosulfate can be

purchased in this form or can be diluted

10 to 1 volumetrically from 0.1N solution.

8.1.4 Adjust solution to pH 7.0 with

sodium carbonate or acetic acid as

necessary.

8.2 Option 1-Accelerated Laundering

Tester:

8.2.1 Place 1000 mL of solution (from

8.1) in the canister of the testing machine.

Adjust temperature to 21°C (70°F).

8.2.2 Place specimen and control fabric

in canister with solution. Specimen size 5

× 5 cm; control fabric size 5 × 5 cm. Total

weight of specimen and control fabric

1.0 ± 0.05 g. Multiple specimens from

the same sample can be used to achieve a

AATCC TM162-2011e2

Test Method for Colorfastness to Water: Chlorinated Pool

Provided by Accuris under license with AATCC

Licensee=Underwriters Laboratories - Ho Chi Ming City, Vie/5909636157, User=Le,

Not for Resale, 11/23/2023 20:10:19 MST

No reproduction or networking permitted without license from Accuris

--``,`,,,``,,```,`,,,,,,`````,-`-`,,`,,`,`,,`---

AATCC Manual of International Test Methods and Procedures/2023 AATCC TM162-2011e2 315

1.0 g load. Place lid with gasket on top of

canister and lock in place. Invert canister

and check for leakage.

8.2.3 The closed canister is placed in

the testing machine with the test speci-

mens and the control fabric at 21°C. Run

each fabric and control fabric separately

for this test. Tumble the specimen with

solution for 60 min. Note: Steel balls are

not added to this solution.

8.3 Option 2-Drycleaning Cylinder

Tester:

8.3.1 Purge the drycleaning cylinder.

Add approximately 5000 mL deionized

water and 0.5 mL household sodium hy-

pochlorite solution (see 11.5). Close cyl-

inder and run for 10 min (purging is nec-

essary only if cylinder has been used for

testing other than chlorinated pool water,

or has not been used for a period of two

weeks). Discard this solution.

8.3.2 Place the 5000 mL solution (from

8.1) in the cylinder of the testing ma-

chine. Adjust temperature to 21°C

(70°F).

8.3.3 Place colored test specimens in-

cluding test control, close and tumble for

60 min.

8.4 For both options, remove the test

specimens and pass through wringer to

remove excess solutions. Rinse thor-

oughly with deionized or distilled water.

Wring again and allow to dry on absor-

bent, bleached paper toweling at room

temperature.

9. Evaluation Method for Color Change

9.1 Classify the change in color of the

Test Control Fabric 162 with the Gray

Scale for Color Change (AATCC EP1) or

AATCC EP7, Instrumental Assessment

of the Change in Color of a Test Speci-

men. If the classification is not equivalent

to a 2-3 or 3, the test is considered to be

invalid. If classification is equivalent to a

2-3 or 3, proceed with 9.2.

9.2 Rate the change in color of test

specimens with the Gray Scale for Color

Change (AATCC EP1), or using AATCC

EP7, and record the numerical rating that

corresponds to the appropriate one on the

Gray Scale (see 11.6 and 11.8).

10. Precision and Bias (see 11.8)

10.1 An interlaboratory study involv-

ing five different laboratories, eight dif-

ferent colored fabric samples, eight con-

trol fabrics, two test methods

(drycleaning cylinder and accelerated

laundering machine) and two colorfast-

ness rating procedures (manual and pho-

tometer) was conducted to define the var-

ious statistical parameters for this test

method. All five laboratories ran the col-

orfastness test on the group of eight fab-

rics using both test methods and both rat-

ing procedures. The main observations of

the study are stated in Table I.

10.1.1 The drycleaning cylinder

method showed a mean fastness rating of

3.483 and the accelerated laundering

method showed a mean fastness rating of

3.3213. The difference between the mean

values was not statistically significant at

95% confidence level.

10.1.2 Manual rating procedure gave a

mean fastness rating of 3.24 while spec-

trophotometer rating gave a mean fast-

ness rating of 3.23. The difference be-

tween the mean values was not statistically

significant at 95% confidence level.

10.1.3 Among the five laboratories,

three laboratories showed very close

mean rating values of 3.249, 3.229 and

3.261. The two outliers showed mean rat-

ing values of 3.415 and 3.055

10.2 Bias. The true value of Colorfast-

ness to Chlorinated Pool Water can only

be defined in terms of a test method.

Within this limitation, this test method

has no known bias.

11. Notes

11.1 Available from Publications Office,

ACGIH, Kemper Woods Center, 1330 Kemper

Meadow Dr., Cincinnati OH 45240; tel: +1.

513.742.2020; web site: www.acgih.org.

11.2 For potential equipment information

pertaining to this test method, please visit

the online AATCC Buyer’s Guide at www.

aatcc.org/bg. AATCC provides the possibility

of listing equipment and materials sold by its

Corporate members, but AATCC does not

qualify, or in any way approve, endorse or cer-

tify that any of the listed equipment or

materials meets the requirements in its test

methods.

11.3 Option 1-Accelerated laundering ma-

chine for rotating closed canisters in a thermo-

statically controlled water bath at 40 ± 2 rpm.

11.4 Option 2-Drycleaning Cylinder; stain-

less steel cylinder of approximately 33 cm (13

in.) high and about 22 cm (8.75 in.) in diame-

ter. The cylinder is mounted in a vertical posi-

tion on an axis inclined 50° and is rotated at a

speed of 45-50 rpm.

11.5 Household sodium hypochlorite solu-

tion. When purchased, the strength will be

5.25% or slightly higher. All sodium hy-

pochlorite solutions lose strength in time.

Strength loss is accelerated by exposure to

light and heat. Do not use after 60 days from

purchase.

11.6 Available from AATCC, P.O. Box

12215, Research Triangle Park NC 27709; tel:

+1.919.549.8141; fax: +1.919.549.8933; e-mail:

ordering@aatcc.org; web site: www.aatcc.org.

11.7 Use a 100 mL sample of test solution.

Add 20 mL of 6N sulfuric acid, 6 mL of 12%

potassium iodide and 3 drops of 1% starch so-

lution. Mix thoroughly; the solution should be

brownish blue color. Back titrate with 0.01N

sodium thiosulfate until the first disappear-

ance of the blue starch indicator color. Calcu-

late the available chlorine as follows:

% available chlorine =

(Specific gravity of household sodium hy-

pochlorite solution is 1.08. Using the above

equation, the use of 1.6 mL of sodium thiosul-

fate in back titration would yield a result of

0.0005% or 5.0 ppm.)

11.8 The precision of this test method is de-

pendent on the combined variability of the

material being tested, the test method itself

and the evaluation procedure utilized.

11.8.1 The precision statement shown in

Section 10 was developed from results ob-

tained by visual and instrumental evaluations

(AATCC EP1 and AATCC EP7).

mL Na thiosulfate 0.01N0.0355××

100 mL sp. gr. Na hypochlorite×

--------------------------------------------------------------------------------------- 100×

Table I—Computed Values of

Precision for Colorfastness Rating

No. of

Specimens

Within

Lab

Between

Lab

3 0.207 0.397

2 0.256 0.487

1 0.357 0.689

Provided by Accuris under license with AATCC

Licensee=Underwriters Laboratories - Ho Chi Ming City, Vie/5909636157, User=Le,

Not for Resale, 11/23/2023 20:10:19 MST

No reproduction or networking permitted without license from Accuris

--``,`,,,``,,```,`,,,,,,`````,-`-`,,`,,`,`,,`---

文档加载中……请稍候！
如果长时间未打开，您也可以点击刷新试试。

下载文档到电脑，查找使用更方便

亲，本站95%以上的标准规范都面向会员免费，办理VIP会员下载更省钱，平均每篇不到2元

立即下载 VIP免费下载

已全部加载

标签： #试验方法 #耐水色牢度 #色牢度试验

摘要：

本标准规范文档《AATCC TM162-2011e2 Test Method for Colorfastness to Water Chlorinated Pool 耐水色牢度试验方法：氯化池》详细规定了用于评估纺织品在氯化游泳池水中颜色稳定性的测试程序，适用于纺织面料及成品在频繁接触含氯消毒水环境下的耐褪色、耐变色性能评价。该标准由美国纺织化学师与染色师协会（AATCC）发布，最新版本为TM162-2011e2，内容涵盖测试样品的制备、氯化池模拟溶液的配制（特定浓度与pH值）、浸泡时间与温度控

展开>> 收起<<

AATCC TM162-2011e2 Test Method for Colorfastness to Water Chlorinated Pool 耐水色牢度试验方法：氯化池.pdf

共2页,预览2页

还剩页未读，继续阅读

声明：本文档系会员上传，若文档所含内容侵犯了您的版权或隐私，请立即通知，我们立即给予侵权申诉删除！

AATCC TM162-2011e2 Test Method for Colorfastness to Water Chlorinated Pool 耐水色牢度试验方法：氯化池

相关推荐

开通VIP享超值会员特权

相关内容

热门标签

举报选择: