AATCC TM107-2022e 耐水色牢度测试方法

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Copyright © 2024 American Association of Textile Chemists and Colorists
AATCC Manual of International Test Methods and Procedures/2025 AATCC TM107-2022e 183
1. Purpose and Scope
1.1 This test method is designed to
measure the resistance to water of dyed,
printed, or otherwise colored textile yarns
and fabrics.
1.2 Distilled water or deionized water
is used in this test method because natural
(tap) water is variable in composition.
2. Principle
2.1 The specimen, backed by multifi-
ber test fabric, is immersed in water and
then subjected to specified conditions of
pressure, temperature and time. After
conditioning, the change in color of the
specimen and the staining of the attached
multifiber test fabric are observed.
2.2 Results are reported as a Gray
Scale for Change and Staining of grade 5
to 1. A grade of 5 represents no color
change and a grade of 1 represents the
most color change.
3. Referenced Documents
3.1 ASTM D1776, Standard Practice
for Conditioning and Testing Textiles
(see 12.1).
4. Terminology
4.1 colorfastness, n.—the resistance of
a material to change in any of its color
characteristics, to transfer of its colo-
rant(s) to adjacent materials or both, as a
result of the exposure of the material to
any environment that might be encoun-
tered during the processing, testing, stor-
age or use of the material.
5. Safety Precautions
NOTE: These safety precautions are
for information purposes only. The pre-
cautions are ancillary to the testing proce-
dures and are not intended to be all inclu-
sive. It is the users responsibility to use
safe and proper techniques in handling
materials in this test method. Manufac-
turers MUST be consulted for specific
details such as material safety data sheets
and other manufacturers recommenda-
tions. All OSHA standards and rules
must also be consulted and followed.
5.1 Good laboratory practices should
be followed. Wear safety glasses in all
laboratory areas.
5.2 Manufacturers safety recommen-
dations should be followed when operat-
ing laboratory testing equipment.
5.3 See 9.1 for safety precautions re-
lated to using a wringer
6. Apparatus and Materials (see 12.2)
6.1 Perspiration tester (with acrylic
plates) (see Figs. 1 and 2).
6.2 Drying oven—convection.
6.3 Cold cut multifiber test fabrics (8
mm [0.33 in.] bands) containing acetate,
cotton, nylon, silk, viscose rayon and
wool shall be used for specimens contain-
ing silk, or (8mm [0.33 in.] bands) con-
taining acetate, cotton, nylon, polyester,
acrylic and wool shall be used for speci-
mens with no silk present (see 12.3).
6.4 Gray Scale for Staining (AATCC
EP2 or EP12) or AATCC 9-Step Chro-
matic Transference Scale (AATCC EP8)
(see 11.4).
6.5 Gray Scale for Color Change
(AATCC EP1 or EP7) (see 12.4).
6.6 Wringer.
6.7 Petri dish with a depth greater than
1.5cm and capable of containing a 6 x 6 ±
0.2 cm test specimen
6.8 Un-dyed adjacent fabric
6.9 White AATCC Textile Blotting Pa-
per (see 12.4).
6.10 Balance with a weighing accuracy
of ± 0.001 g.
7. Test Solution
7.1 Distilled water or deionized water
from an ion-exchange device.
8. Test Specimens
8.1 Number and size of specimens
8.1.1 For fabric testing, one specimen, 6
x 6 ± 0.2 cm, is needed. Attach a 5 x 5 ±
0.2 cm multifiber test fabric swatch to the
face of the fabric by sewing a single seam
stitch along one edge of the fabric.
8.1.2 For yarn or loose fiber testing,
weigh a 5 × 5 ± 0.2 cm piece of multifi-
ber fabric and a 6 × 6 ± 0.2 cm piece of
the un-dyed adjacent fabric together.
Then take a mass of the yarn or loose fi-
ber approximately equal to one half of the
combined mass of the adjacent fabrics.
Place it between a 5 × 5 ± 0.2 cm piece of
multifiber fabric and a 6 × 6 ± 0.2 cm
piece of the un-dyed adjacent fabric, and
sew a single seam stitch along all four
sides.
9. Procedure
9.1 Weigh each test specimen (as pre-
pared in 8.1) to the nearest 0.1g. Immerse
the test specimen in a petri dish in the test
solution which is at room temperature
with occasional agitation to ensure thor-
ough wetting out (approximately 15 min
generally required for average fabrics).
For fabrics hard to wet out, immerse the
test specimen in the test solution at room
temperature, pass through squeeze rolls
(wringer) and re-immerse. Repeat, if nec-
essary, to attain thorough wetting out.
When using the wringer, ensure adequate
guard at the nip point. Normal safeguards
on pad should not be removed.
9.2 Remove the test specimen from the
test solution and pass each test specimen
assembly through the wringer with the
multifiber stripes perpendicular to the
length of the wringer rolls (all stripes go
through the wringer at the same time).
Weigh each test specimen to be sure it
weighs greater than or equal to 2.5 times
its original weight. Whenever possible,
the wet weight should be 2.5-3.0 times
the original weight. Because certain fab-
rics may not be able to retain this amount
of solution when passing through a
wringer, such fabrics may be tested after
blotting to the required wet pickup with
White AATCC Textile Blotting Paper
(see 12.4).
9.3 Place the test specimen assembly
between acrylic plates and insert in the
specimen unit of the perspiration tester
with the multifiber stripes running per-
pendicular to the long dimension of the
plate (see Fig. 3).
9.4 Depending upon equipment avail-
able, use the following alternates:
9.4.1 Horizontal Perspiration Tester
(see Fig. 1): Place the plates in the perspi-
ration tester with the specimen assem-
AATCC TM107-2022e
Test Method for Colorfastness to Water
Fig. 1—Horizontal perspiration tester.
Copyright AATCC International
Provided by Accuris under license with AATCC
No reproduction or networking permitted without license from Accuris Not for Resale, 2025-04-14 18:24:10 UTC
Sold to: Nawal Analytical Labs India Private limited
Order Number: 00015024
Copyright © 2024 American Association of Textile Chemists and Colorists
184 AATCC TM107-2022e AATCC Manual of International Test Methods and Procedures/2025
blies evenly distributed between the 21
plates. Place all 21 plates into the unit re-
gardless of the number of specimens. Af-
ter placing the final plate in position (on
top) set the dual plates with compensat-
ing springs in position, place the 3.63 kg
(8.0 lb) weight on top making a total of
4.54 kg (10.0 lb) under the pressure plate,
and lock the pressure plate in position by
turning the thumb screws. Remove the
weight and place the unit lying on its side
in the oven so that the sides of the perspi-
ration tester are parallel to the oven walls
(see Fig. 4).
9.4.2 Vertical Perspiration Tester (see
Fig. 2): Assemble the plates in the perspi-
ration tester with the specimens evenly
distributed between the 21 plates. Place
all 21 plates into the unit regardless of the
number of specimens. The plates are held
in a vertical position between an indicat-
ing scale with a fixed metal plate at one
end and an adjustable metal plate at the
other end. Use the adjusting screw to ex-
ert a 4.54 kg (10.0 lb) force against the
plates. Lock the specimen unit containing
the test specimens with a set screw. Re-
move the pressure gauge unit from the
specimen unit and place the specimen
unit in the oven such that the side of the
perspiration tester is to the oven walls.
Another specimen unit may be added to
the pressure gauge unit and the loading
procedure repeated.
9.5 Heat the loaded specimen unit in an
oven at 38 ± 1°C (100 ± 2°F) for 18 h ± 5
min.
9.6 Remove the tester from the oven
and for each test specimen assembly, sep-
arate the multifiber fabric and, if used,
the adjacent fabric from the test fabric.
Place the multifiber fabric and test fabric
specimens separately on a wire screen in
accordance with ASTM D1776 over-
night.
10. Evaluation
10.1 Color Change.
Fig. 2—Vertical perspiration tester.
Fig. 3—Specimen in holder.
Fig. 4—Horizontal perspiration tester placement in oven.
Copyright AATCC International
Provided by Accuris under license with AATCC
No reproduction or networking permitted without license from Accuris Not for Resale, 2025-04-14 18:24:10 UTC
Sold to: Nawal Analytical Labs India Private limited
Order Number: 00015024
Copyright © 2024 American Association of Textile Chemists and Colorists
AATCC Manual of International Test Methods and Procedures/2025 AATCC TM107-2022e 185
10.1.1 Evaluate the test specimen for
change in color by comparison with the
Gray Scale for Color Change (AATCC
EP1), or by using Instrumental Assess-
ment of the Change in Color of a Test
Specimen (AATCC EP7), and record the
numerical rating that corresponds to the
appropriate one on the Gray Scale.
10.2 Staining (see 12.7).
10.2.1 Evaluate the staining of the mul-
tifiber fabric used (see 12.5) by compari-
son with the Gray Scale for Staining
(AATCC EP2), the AATCC 9-Step Chro-
matic Transference Scale (AATCC EP8),
or Instrumental Assessment of Degree of
Staining (AATCC EP12), and record the
numerical rating that corresponds to the
appropriate one on either of them. Report
which scale was used (see 12.6).
11. Precision and Bias
11.1 Precision. Proficiency data gener-
ated by 91 different labs during five dif-
ferent time periods (June 2012, Decem-
ber 2012, June 2013, December 2013 and
June 2014) was used to define the preci-
sion of stain rating and color change rat-
ing values. Each lab used the same fabric
materials to obtain the stain rating and
color change rating values. Each lab per-
formed three replicate tests for each test
material and used three different raters to
assign ratings for staining and color
change. Each lab also used multi-fiber
fabric strips containing acetate, acrylic,
cotton, nylon, polyester and wool fibers
to assess the staining of individual fibers.
11.1.1 Tables I-VI give the within lab
and between lab precision values for the
stain ratings of acetate, acrylic, cotton,
nylon, polyester and wool fibers.
11.1.2 Table VII gives the precision
values for color change rating. As men-
tioned above, the multi-period data gen-
erated by 91 different labs was used to
compute the precision values.
11.1.3 In addition to providing the pre-
cision values, the analysis of the multi-
period data revealed the following statis-
tical facts:
The stain ratings assigned by different
labs for acetate fiber differed signifi-
cantly at 95% confidence level.
The mean stain ratings of acetate fiber
corresponding to five different time pe-
riods differed significantly at 95% con-
fidence level.
The stain ratings assigned by different
labs for acrylic fiber differed signifi-
cantly at 95% confidence level.
The mean stain ratings of acrylic fiber
corresponding to five different time pe-
riods differed significantly at 95% con-
fidence level.
The stain ratings assigned by different
labs for cotton fiber did not differ sig-
nificantly at 95% confidence level.
The mean stain ratings of cotton fiber
corresponding to five different time pe-
riods differed significantly at 95% con-
fidence level.
The stain ratings assigned by different
labs for nylon fiber did not differ sig-
nificantly at 95% confidence level.
The mean stain ratings of nylon fiber
corresponding to five different time pe-
riods differed significantly at 95% con-
fidence level.
The stain ratings assigned by different
labs for polyester fiber differed signif-
icantly at 95% confidence level.
The mean stain ratings of polyester fi-
ber corresponding to five different time
periods differed significantly at 95%
confidence level.
The stain ratings assigned by different
labs for wool fiber did not differ sig-
nificantly at 95% confidence level.
The mean stain ratings of wool fiber
corresponding to five different time pe-
riods differed significantly at 95% con-
fidence level.
•The mean color change ratings of dif-
ferent labs did not differ significantly
at 95% confidence level. The mean
color change ratings of five different
time periods differed significantly at
95% confidence level.
In general the between period variation
was more than the between lab variation.
11.2 Bias. Colorfastness to water can
be defined only in terms of a test method.
There is no independent method for de-
termining the true value. As a means of
estimating this property, the method has
no known bias.
Table I—Precision Table for
Stain Rating of Acetate
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.02879 0.03715
2 0.0204 0.0263
3 0.0166 0.0214
4 0.0144 0.0186
5 0.0129 0.0166
6 0.0118 0.0152
Table II—Precision Table for
Stain Rating of Acrylic
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.02983 0.03849
2 0.0211 0.0273
3 0.0172 0.0222
4 0.0149 0.0192
5 0.0133 0.0172
6 0.0122 0.0157
Table III—Precision Table for
Stain Rating of Cotton
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.11251 0.14512
2 0.0797 0.1028
3 0.0650 0.0838
4 0.0563 0.0726
5 0.0503 0.0649
6 0.0459 0.0592
Table IV—Precision Table for
Stain Rating of Polyester
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.06906 0.08911
2 0.0489 0.0631
3 0.0399 0.0514
4 0.0345 0.0446
5 0.0309 0.0399
6 0.0282 0.0364
Table V—Precision Table for
Stain Rating of Polyester
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.03017 0.03894
2 0.0214 0.0276
3 0.0174 0.0225
4 0.0151 0.0195
5 0.0135 0.0174
6 0.0123 0.0159
Table VI—Precision Table for
Stain Rating of Wool
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.03743 0.04831
2 0.0265 0.0342
3 0.0216 0.0279
4 0.0187 0.0242
5 0.0167 0.0216
6 0.0153 0.0197
Table VII—Precision Table for Color
Change Rating
No. of
Specimens
Within Lab
Precision
Between Lab
Precision
1 0.04181 0.05376
2 0.0296 0.0381
3 0.0241 0.0310
4 0.0209 0.0269
5 0.0187 0.0240
6 0.0171 0.0219
Copyright AATCC International
Provided by Accuris under license with AATCC
No reproduction or networking permitted without license from Accuris Not for Resale, 2025-04-14 18:24:10 UTC
Sold to: Nawal Analytical Labs India Private limited
Order Number: 00015024
摘要:

本页面详细介绍AATCC TM107-2022e标准,即纺织品耐水色牢度的测试方法。该标准由美国纺织化学师与印染师协会(AATCC)发布,是评估纺织面料在水中颜色转移程度的重要国际测试规范。最新版标准(2022e)明确了试样制备、水浴处理、干燥与评级等关键步骤,适用于检验服装、家纺及工业用纺织品在浸水条件下的色牢度性能。掌握该测试方法有助于企业控制产品质量、满足出口合规要求,并为采购商和检测机构提供可靠的参考依据。

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