ASTM D2457 - 21

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Carl 2024-09-03 58 177.16KB 6 页 10星币
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Designation: D2457 21
Standard Test Method for
Specular Gloss of Plastic Films and Solid Plastics
1
This standard is issued under the fixed designation D2457; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This test method describes procedures for the measure-
ment of gloss of plastic films and solid plastics, both opaque
and transparent. It contains four separate gloss angles (Note 1):
1.1.1 60-deg, recommended for intermediate-gloss films,
1.1.2 20-deg, recommended for high-gloss films,
1.1.3 45-deg, recommended for intermediate and low-gloss
films,
1.1.4 85-deg, recommended for intermediate and low gloss
films, and
1.1.5 75-deg, recommended for plastic siding and soffit.
NOTE 1—The 85-deg, 75-deg, 60-deg, and 20-deg apparatus and
method of measurement duplicate those in Test Method D523 and D3679;
those for the 45° procedure are similarly taken from Test Method C346.
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
NOTE 2—There is no known ISO equivalent to this standard.
1.3 This international standard was developed in accor-
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
2
C346 Test Method for 45-deg Specular Gloss of Ceramic
Materials
D523 Test Method for Specular Gloss
D3679 Specification for Rigid Poly(Vinyl Chloride) (PVC)
Siding
E284 Terminology of Appearance
E691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
E1347 Test Method for Color and Color-Difference Mea-
surement by Tristimulus Colorimetry
E1349 Test Method for Reflectance Factor and Color by
Spectrophotometry Using Bidirectional (45°:0° or 0°:45°)
Geometry
E2935 Practice for Conducting Equivalence Tests for Com-
paring Testing Processes
3. Terminology
3.1 Definitions—For definitions of terms used in this test
method, see Terminology E284.
4. Significance and Use
4.1 Specular gloss is used primarily as a measure of the
shiny appearance of films and surfaces. Precise comparisons of
gloss values are meaningful only when they refer to the same
measurement procedure and same general type of material. In
particular, gloss values for transparent films should not be
compared with those for opaque films, and vice versa. Gloss is
a complex attribute of a surface which cannot be completely
measured by any single number.
4.2 Specular gloss usually varies with surface smoothness
and flatness. It is sometimes used for comparative measure-
ments of these surface properties.
5. Apparatus
5.1 Instrumental Components—Each apparatus (Note 3)
shall consist of an incandescent light source furnishing an
incident beam, means for locating the surface of the specimen,
and a receptor located to receive the required pyramid of rays
reflected by the specimen. The receptor shall be a photosensi-
tive device responding to visible radiation.
NOTE 3—The 75-, 60-, and 20-deg procedures require apparatus
identical to that specified in Test Method D523. The 45° procedure
requires apparatus like that specified in Test Method C346.
5.2 Geometric Conditions—The axis of the incident beam
shall be at one of the specified angles from the perpendicular to
the specimen surface. The axis of the receptor shall be at the
mirror reflection of the axis of the incident beam. With a flat
piece of polished black glass or other front-surface mirror in
1
This test method is under the jurisdiction of ASTM Committee D20 on Plastics
and is the direct responsibility of Subcommittee D20.40 on Optical Properties.
Current edition approved May 1, 2021. Published June 2021. Originally
approved in 1965. Last previous edition approved in 2013 as D2457 13. DOI:
10.1520/D2457-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1
specimen position, an image of the source shall be formed at
the center of the receptor field stop (receptor window). The
length of the illuminated area of the specimen shall be equal to
not more than one third of the distance from the center of this
area to the receptor field stop. The angular dimensions and
tolerances of the geometry of the source and receptor shall be
as indicated in Table 1. The angular dimensions of the receptor
field stop are measured from the center of the test surface. The
angular dimensions of the source field stop are mostly easily
measured by the specimen-to-window angular size of the
mirror image of the source formed in the receptor field stop.
(See Fig. 1 for a generalized illustration of the dimensions.)
The tolerances are chosen so that errors of no more than one
gloss unit at any point on the scale will result from errors in the
source and receptor aperture.
5.3 Vignetting—There shall be no vignetting of rays that lie
within the field angles specified in 5.2.
5.4 Spectral Conditions—Results should not differ signifi-
cantly from those obtained with a source-filter-photocell com-
bination that is spectrally corrected to yield CIE luminous
efficiency with CIE Source C. Since specular reflection is, in
general, spectrally nonselective, spectral corrections need be
applied only to highly chromatic, low-gloss specimens upon
agreement of users of this test method.
5.5 Measurement Mechanism—The receptor-measurement
mechanism shall give a numerical indication that is propor-
tional to the light flux passing the receptor field stop within 61
percent of full-scale reading.
6. Reference Standards
6.1 Primary Working Standards may be highly polished,
plane, black glass surfaces. The specular reflectance, in
percent, (R
s
) of such surfaces shall be computed by the
following equation:
R
s
~
percent
!
5(1)
50
FF
cos i2
=
n
2
2sin
2
i
cos i1
=
n
2
2sin
2
i
G
2
1
F
n
2
cosi2
=
n
2
2sin
2
i
n
2
cosi1
=
n
2
2sin
2
i
G
2
G
where:
i= the specular (incidence) angle, and
n= the index of refraction of the surface.
Multiply the computed R
s
at each angle by the scale factors
shown in Table 2.
NOTE 4—On the 45 and 60° scales, a perfect mirror measures 1000.
6.2 Secondary Working Standards of ceramic tile, glass,
porcelain enamel, or other materials having hard, flat, and
uniform surfaces may be calibrated from the primary standard
on a glossmeter determined to be in strict conformance with the
requirements prescribed in 5.2.
7. Preparation and Selection of Test Specimens
7.1 This test method does not cover preparation techniques.
Whenever a test for gloss requires the preparation of a test
specimen, report the technique of specimen preparation.
7.2 Test results have been found to be seriously affected by
surface warpage, waviness, or curvature. Ensure that specimen
surfaces have good planarity. Perform tests with the directions
of machine marks, or similar texture effects, both parallel and
perpendicular to the plane of the axes of the incident and
reflected beams, unless otherwise specified. (Note that this
does not avoid the second-surface reflection.)
7.3 Surface test areas shall be kept free of soil and abrasion.
Gloss is due chiefly to reflection at the surface; therefore,
anything that changes the surface physically or chemically is
likely to affect gloss.
8. Mounting Films for Measurement
8.1 Any nonrigid film must be mounted in a device that will
hold it flat, but will not stretch the film while it is measured.
Three different filmholding devices have each proved satisfac-
tory for at least some types of films:
8.1.1 Vacuum Plate (see Fig. 2) is required for stiff films.
Connect the vacuum plate by rubber tube to a vacuum pump or
vacuum line. With thin, soft films it is sometimes necessary to
use a valve and pressure gage and to limit the vacuum so as to
keep from collapsing the soft film into the pores of the ground
plate.
8.1.2 Flat Plate with two-side pressure-sensitive tape (see
Fig. 3). Make sure each specimen is pulled smooth, but not
stretched before holding it by the two strips of adhesive tape.
Replace the tape whenever it loses its adhesiveness.
8.1.3 Telescoping Ring or Hoop (see Fig. 4)To mount the
specimen in the telescoping ring, lay the flexible film over the
base (male) section and drop the top over the base. Push down
carefully, taking care to pull the test film taut without stretching
it. Measure the taut area.
8.2 Backing for Films That Transmit Light—A matt black
backing or (even better) a black cavity must be placed behind
any film that transmits light. Erroneous measurements will
occur without a suitable trap or backing.
TABLE 1 Angular Dimensions and Tolerances of Geometry of Source and Receptor Field Stops
Source Field Stop Receptor Field Stop
Geometry, deg Incidence Angle, deg In Plane of Measurement,
deg
Perpendicular to Plane of
Measurement, deg In Plane of Measurement, deg Perpendicular to Plane of
Measurement, deg
75 75 ± 0.1 3.0 max
60 60±0.1 0.75±0.25 3.0max 4.4±0.1 11.7±0.2
20 20 ± 0.1 0.75 ± 0.25 3.0 max 1.80 ± 0.05 3.6 ± 0.1
45 45±0.1 1.4±0.4 3.0±1.0 8.0±0.1 10.0±0.2
D2457 − 21
2
9. Procedure
9.1 Operate the glossmeter in accordance with the manufac-
turer’s instructions.
9.2 Calibrate the instrument at the start and completion of
every period of glossmeter operation and during the operation
at sufficiently frequent intervals to assure that the instrument
response is practically constant. If at any time an instrument
fails to repeat readings of the standard to within 2 percent of
the prior setting, the intervening results should be rejected. To
calibrate, adjust the instrument to read correctly the gloss of a
highly polished standard, and then read the gloss of a standard
having poorer image-forming characteristics. If the instrument
reading for the second standard does not agree within 1 percent
of its assigned value, do not use the instrument without
readjustment, preferably by the manufacturer.
NOTE 5—Correct readings on black-glass and intermediate standards do
FIG. 1 Diagram of Glossmeter Showing Essential Components and Dimensions
TABLE 2 Scale Factors for Gloss Standards, Perfect Mirror and Perfect Matt White
A
Geometry
Scale Factors (multiply
R
s
of black glass
standard by)
Value for Black Glass when
n= 1.540 Value for Perfect Mirror Value for Perfect Matt White
60° 10.0 95.8 1000 2.1
20° 20.3 92.3 2030 1.4
45° 10.0 55.9 1000 5.4
A
The latter are useful for estimating corrections to gloss readings for reflection from sample backing (see Note 6).
FIG. 2 Vacuum Plate Used to Hold Films Flat
D2457 − 21
3
摘要:

ASTM D2457 - 21 是当前最新版本的 ASTM 标准规范,专门用于测定塑料薄膜与固体塑料表面的镜面光泽度。该标准通过采用 20°、45° 或 60° 等不同几何角度的入射光,量化材料表面的反射特性,适用于透明、半透明及不透明塑料制品的光泽度评估。规范详细规定了仪器校准、样品制备、测试步骤及数据处理方法,确保实验室间结果的重复性与可比性。对于塑料薄膜、板材、注塑件及涂层表面,ASTM D2457 - 21 为质量控制和产品开发提供了关键的光学性能指标,广泛应用于包装、汽车内饰、电子外壳

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作者:Carl 分类:国外协会 价格:10星币 属性:6 页 大小:177.16KB 格式:PDF 时间:2024-09-03

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