ASTM RR-C09-1008 1994

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This Research Report is issued under the fixed designation RR: C09-1008. You agree not to reproduce or circulate or quote, in whole or
part, this document outside of ASTM International Committee/Society activities, or submit it to any other organization or standards
body (whether national, international or other) except with the approval of the Chairman of the Committee having jurisdiction and the
written authorization of the President of the Society. If you do not agree to these conditions, please immediately destroy all copies of
this document. Copyright ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428. All rights reserved.
6 June 1994
Committee C09 on Concrete and Concrete Aggregates
Subcommittee C09.24on Supplementary Cementitious Materials
Research Report C09-1008
Interlaboratory Study to Establish Precision Statements for ASTM
C311, Tests for Sampling and Testing Fly Ash or Natural Pozzolans for
Use as a Mineral Admixture in Portland Cement Concrete
Technical contact:
Toy S. Poole
Department of the Army
Waterways Experiment Station
Corp of Engineers
3909 Halls Ferry Rd
Vicksburg, MS
Email: tovs.poole@usace.armv.mil
Tel: 601-634-3261
ASTM International
100 Barr Harbor Drive
West Conshohocken, PA 19428-2959
DEPARTMENT
OF
THE
ARMY
WATERWAYS
EXPERIMENT
STATION,
CORPS
OF
ENGINEERS
3909
HALLS
FERRY
ROAD
VICKSBURG,
MISSISSIPPI
39180-6199
REPLY
TO
ATTENTION
OF
August
5,
1993
CEWES-SC
Mr.
W.
Scott
Orthey
ASTM
1916
Race
Street
Philadelphia,
PA
19103-1187
Scott:
OTv.
PWiPT^!
V/TTJ;
»
AUG
0
9
1993
AST
M
Enclosed
is
the
report
I
wrote
from
which
a
precision
and
bias
statement
for
C
311
(C09.24)
was
developed.
Craig
Cain
asked
me
to
send
it
to
you
since
this
item
is
now
at
the
ballot
step
at
which
a
report
number
is
appropriately
assigned.
Please
let
me
know
if
additional
things
are
needed.
Sincerely,
end
Toy
S.
Poole
Concrete
Technology
Division
(yijOQJUo^jcJk-
(jfcz&r
•
HYDRAULICS
LABORATORY
GEOTECHNICAL
LABORATORY
STRUCTURES
LABORATORY
ENVIRONMENTAL
LABORATORY
COASTAL
ENGINEERING
RESEARCH
CENTER
INFORMATION
TECHNOLOGY
LABORATORY
Results
of
Interlaboratory
Study
to
Determine
the
Precision
and
Bias
of
Chemical-Analysis
Methods
Described
in
ASTM
C
311
Toy
S.
Poole
Waterways
Experiment
Station,
Vicksburg,
MS
INTRODUCTION
ASTM
C
311
essentially
relies
on
ASTM
C
114
for
methods
for
the
determination
of
chemical
composition
of
coal
fly
ash,
but
the
latter
document
does
not
purport
to
be
applicable
to
materials
other
than
hydraulic
cements,
and
therefore
its
estimates
of
precision
and
bias
are
not
applicable
to
coal
fly
ash.
The
purpose
of
this
report
is
to
report
the
results
of
an
interlaboratory
study
conducted
in
1987-89
for
the
purposes
of
developing
these
estimates.
Seven
laboratories
participated
in
the
study:
Ash
Grove
Cement
Co.;
Cal-Mat
Co.;
Dundee
Cement
Co.;
General
Portland,
Inc.;
Resource
Materials
Testing,
Luc;
Riverside
Cement
Co.;
Waterways
Experiment
Station.
MATERIALS
AND
METHODS
National
Institute
for
Standards
and
Technology
(NIST)
Standard
Reference
Materials
(SRM's)
coal
fly
ash
samples
2689,
2690,
2691,
and
1633a
were
used
in
the
program.
Participants
were
instructed
to
complete
analyses
according
to
ASTM
C
311-87.
These
methods
are
basically
ASTM
C
114
reference
methods
for
the
chemical
analysis
of
hydraulic
cements
for
which
insoluble
residues
exceed
1%.
The
C
114
method
for
determination
of
Fe^
has
been
changed
since
this
interlaboratory
work
was
done.
Therefore,
precision
and
bias
estimates
for
this
method,,
which
were
developed
and
reported
by
Richter
and
Poole
(1992),
are
substituted
for
the
results
obtained
in
the
interlaboratory
study.
RESULTS
Results
reported
by
each
laboratory
are
summarized
in
Table
1,
along
with
simple
descriptive
statistics.
Laboratory
identification
numbers
are
not
related
to
the
sequence
in
which
laboratories
were
identified
above.
All
data
and
descriptive
statistics
are
reported
to
two
decimal
places.
There
was
no
substantial
evidence
that
any
data
needed
to
be
removed
because
of
variances
that
were
too
high
of
too
low,
as
described
in
C
802.
There
were
a
few
instances
in
which
a
particular
set
of
analyses
were
associated
with
a
variance
that
e^jJl
摘要:

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作者:Carl 分类:国外协会 价格:10星币 属性:21 页 大小:408.31KB 格式:PDF 时间:2024-09-05

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